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S310.00g228.49mmol250mL50mL1510mol/L3.5mL4hTLCS3: Add 10.00g of intermediate 2 (28.49mmol) into a 250mL reaction flask, add 50mL of methanol, slowly add 3.5mL of 10mol/L sodium hydroxide solution at a temperature of 15C, after the addition is complete, keep the reaction for 4 hours, observe on a TLC plate, The response is complete

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