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To a stirred solution of 3-bromo-5-(difluoromethoxy)-2-(difluoromethyl)pyridine (0.98 g, 3.6 mmol), bis(pinacolato)diboron (1.82 g, 7.2 mmol), PdCl 2 (dppf) (263 mg, 0.36 mmol), and dioxane (12 ml) was added KOAc (1.06 g, 10.8 mmol)

1 H chemical shifts are expressed in ppm using the residual non-deuterated solvent as an internal standard, and the coupling constants J are specified in Hz

for C 36 H 45 N 6 O 8 S 3 + [M + H] + , 785.25

I purchase a lot of Pure Encapsulations products every year, and have done so for many years, and in the last 6 months or so Ive noticed a musty smell to their capsules

doi:10.1016/j.pscychresns.2021.111302 114. Sohal, V

Yousefi M, Narmani A, Jafari SM